Decarboxylation Package – Ai 100L Jacketed Glass Reactor

$79,866.70

Ai R-series single/dual jacketed glass reactors are designed for synthetic reaction of different types of materials in a controlled temperature and vacuum environment. Each reactor features adjustable stirring speeds and a constant pressure feeding funnel that allows you to add material to the vessel at a uniform and controlled speed. The built-in condenser makes it possible to recover some materials, also at a controlled rate of speed.

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SKU: R100-UnistatT305-2163 Category: Brand:

Description

Ai R-series single/dual jacketed glass reactors are designed for synthetic reaction of different types of materials in a controlled temperature and vacuum environment. Each reactor features adjustable stirring speeds and a constant pressure feeding funnel that allows you to add material to the vessel at a uniform and controlled speed. The built-in condenser makes it possible to recover some materials, also at a controlled rate of speed.

Features

  • ETL tested to UL and CSA standards (optional)
  • Now includes a FREE high quality thermo insulation jacket (a $779 value) with open/close viewing window and top/bottom adjustable drawstrings, specially designed and made for Ai glass jacketed reactors. These jackets will extend chiller life, allow you to go down to a lower temperature, and also cut your utility bill.
  • Solvent-resistant PTFE on all sealing components ensures long time durability and operation.
  • All glassware is hand-made from food grade high borosilicate glass that is heat/cold/corrosion-resistant.
  • Adjustable stirring rate provides great torque or high speed.
  • Patented PTFE stirring rod bearing for reliable and quiet operation.
  • Optional multi-layer stirring blades for optimal reaction results.
  • Wide range of temperature operations, from -110F to 400F.
  • Large condenser cooling surface for exceptional condensation performance.
  • Rugged stainless steel reinforced PTFE stirrer with anchored agitator, suitable for a wide range of viscous materials.
  • Easily visual operation with digital speed and temperature displays.
  • Heavy duty stainless steel supporting framework with lockable casters for mobility and stability. (whole support and glass vessel shipped pre-assembled)
  • One year warranty and lifetime US-based parts, service, and support.

Your safety is important to us! Please use caution when operating. Users of glass reaction equipment must take all necessary precautions to avoid contact with rotating parts, particularly entanglement of loose clothing, hair, necklaces, or other jewelry. Under these circumstances, the winding action of the rotating parts can draw the user(s) into the apparatus, resulting in breakage of glassware, burns, and/or chemical exposure. Extra caution must also be taken when operating with air-reactive materials, especially under vacuum. A leak can draw air into the apparatus and cause a violent reaction to occur.

 

FAQ for Glass Reactor Series

 

  1. When do you recommend using the different impeller types that you have listed on the website?
    The two different impeller types that we have is the pitched blade and the anchor agitator. It is recommended to use the pitched impeller for low viscosity solutions such as aqueous solutions and organic solvents. The anchor impeller is best used for higher viscosity applications such as thick oils, resins, and polymers.
  2. How do I clean my reactor?
    The most effective and efficient way to clean your reactor would be by using the clean in place kit shown below paired with a pump capable of achieving between 10-20 psi.
  3. What is the best way to fill the reactor?
    The best way to fill the reactor is to pull vacuum on the reactor from the condenser, and use either the stopcock on the lid or other fitting connected to a hose to pull the suck fluid into the reactor. As long as the other end of the tube is submerged in liquid and the pressure inside of the reactor is less than atmospheric pressure, fluid will enter the reactor.

  4. What are the materials of construction for the reactor’s wetted parts?
    3 borosilicate glass and PTFE
  5. How long is the warranty period and what does it cover?
    The length of the warranty is one year, and it covers manufacturing defects,
  6. What accessories come with the reactor?
    The reactor will come with everything listed on the standard package for the unit that will be purchased. If purchasing an entire turnkey, please see the turnkey’s standard package. The standard package can be found on the web listing at Across International’s website under the standard package tab.
  7. Where can I find technical information about the Across International reactor?
    Technical information can be found on the Across International website under the specifications tab. If further technical information is needed, please reach out to the sales team via email or phone at Across International: [email protected] or 888-980899.
  8. What are the lid port sizes for my glass reactor?
    The lid port sizes will vary depending on reactor type. Any port not labelled on the drawing is specific to Across International, take note that the QC-35 is also specific to Across International but clamps and adapters can be bought from Across International as needed for all lid adapters.

    Lid for 10-50L reactor:

    Lid for 100L-200L reactor:

  9. Will these sizes fit standard American ground glass joints? If so which ones will fit?
    Please see the table below for a detailed description of which Across International glass reactor joints will fit the standard American ground glass joints:

Across International Joints Conical Joints

Compatible American Standard Conical Joints

40/38

40/50

34/35

34/45

24/29

24/40

14/23

14/35

 

Specifications

Specifications

ModelR100
Electrical requirements
110V 60Hz or 220V 50/60Hz, 1-Phase, 250W
Reaction glass vessel capacity
26 gallons (100L)
Cooling/heating jacket capacity
8 gallons (30L)
Glass materialHigh borosilicate glass 3.3
Rotation controllerDigital controller with variable frequency drive
Rotation speed: 50 to 500 rpm
Maximum jacket pressure
4.4 psi or 0.03 MPa
Drain valveFlush seal design with large opening and flat flange clamp
AgitatorStyle: impeller
Material: 304 stainless steel with PTFE liner
FunnelPressure equalizing
Vacuum gaugeMechanical
Swivel casterFour
Glass vessel temperature range
-110F to 400F
Vacuum level20 torr
Vacuum sealingGlass or PTFE
Drain port ground clearance
13.5 inches
Unit dimesions (WxDxH)28 x 42 x 95"
Shipping dimensions26 x 88 x 45"
Shipping weight460s
ComplianceETL tested to UL and CSA standards
Standard Packages

R100-UnistatT305-2163 Standard package with all optional parts

 Part description

 Quantity

Part image

 Huber Unistat T305 +300C system1 set 
 Jacketed glass vessel, lid, clamps and heavy duty stainless steel stand with casters (shipped pre-assembled)
1 set
 Glass vessel insulation jacket with openable viewing window1 pc 

 Vertical condenser with dual cooling coils, 2 chilling fluid ports and 1 vacuum port, glass

1 pc
 Glass condenser dispenser with drain port and PTFE open/close valve
1 set
 Glass feeding funnel with PTFE open/close valve
1 set
 Glass receiving flask with PTFE open/close valve1 set
 1" glass drain port with PTFE open/close valve
1 set
 Glass vacuum valve
6 sets
 Stirring motor controller with material temperature display
1 pc
 Stirring motor and motor support
1 set 
 Mechanical vacuum gauge with two 3/8" hose barb ports
1 pc
 Temperature probe with PTFE seal
1 pc
 PTFE stirring blades, stainless steel rod with PTFE liner
1 pc

 Insulated hose with drain port & open/close valve x 2
 3/8" Stainless steel hose barb adapters x 2

4 pcs
 
 PTFE sealing tape1 pc 
 PTFE stirring rod positioner/bearing kit
1 set
 Condenser dispenser connection kit1 set
 Large opening material feeding port kit1 set
 Bottom drain port sealing clamp 1 set
 Rubber-wrapped condenser dispenser support and condenser bracket3 pcs
 Chilling fluid connector x 2, vacuum connector x 1
3 sets
 Allen key and backup inner hex screws1 set
 Users manual1 pc

 

Welch 2163 Pump Standard package

 Part description

 Quantity

Part image

 Welch 2163 6.1 cfm 8-head diaphragm pump
1 pc

 Threaded Hose Barbs (Welch PN: 710798)2 pc

 Pneumatic Plastic Muffler
1 pc

 Power Cord with Plug1 pc

 12 mm diameter EDPM O-ring (Welch PN 829217-3)2 pc

 User's manual1 pc

 

Huber Unistat T305 Package

 Part description

 Quantity

Part image

HUBER Unistat T305 300°C with Pilot ONE - 208V1 pc

Mini-USB Cable1 pc

M16X 1 to M24 x 1.5 Adapters4 pc

 Huber expansion tank, adapters, tubing and fluid
  6161 x 1     M20 (-20 to 195)   5L
  6162 x 3     M20 (-20 to 195) 10L
  9256 x 2     90° Adaptor M24x1,5female-M24x1,5male
  9327 x 2     2m     (-60 to 260) tubing
  9825 x 2     M24 X 1.5 (male) to 3/4" NPT (male)
  10967 x 1   5L expansion tank
1 set 
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